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HANDBOOK OF SYNTHETIC ORGANIC CHEMISTRY 2

Chemistry

Mathematics & Science

Gt Product Group

Binding Format

Marketing Imprint Name

B2B GT

CL Carton Count

Imprint Name

B2B & B2C

This handbook provides practical guidance for planning, working up, documenting, analyzing, and improving reactions in synthetic organic chemistry. It includes coverage on important topics such as lyophylization, crystallization, precipitation, HPLC detectors, gases, and microwave reactions. The book maintains the useful organization of the author’s earlier work, beginning with a basic overview and walking through every practical step of the process of organic synthesis, from reagents, solvents, and temperature control, to documentation, implementation, purification, and analytical methods for the product. From planning and setting up reactions, to recording them, the book provides insight and valuable guidance into every step of the process.

Handbook of Synthetic Organic Chemistry

COLFR

COLSO

COLJR

COLSR

Duration

Duration Unit Of Measure

Transaction Type

Front Cover.
Half Title Page.
Title Page.
Copyright Page.
Contents.
Foreword.
Preface to the First Edition.
Preface to the Second Edition.
Acknowledgments.
1: Safety.
2: Searching the Literature.
3: Reagents.
4: Gases.
5: Reactions on a Small Scale&#x2014;1&#x2013;25 mmol.
6: Temperature Control.
7: Solvents.
8: The Research Notebook.
9: Conducting the Reaction Itself.
10: Following the Reaction.
11: Working Up Reactions.
12: Evaporation.
13: Vacuum Systems.
14: Purification of Products.
15: Methods for Structure Elucidation.
16: Cleaning Up After the Reaction.
17: Specific Example.
18: Strategies for Reaction Optimization Chapter Outline.
Appendix 1 Safety Protocols.
Appendix 2 Synthetic Solvent Selection Chart.
Appendix 3 Solvent Miscibility.
Appendix 4 Freezing Points of Common Organic Solvents.
Appendix 5 Toxicities of Common Organic Solvents.
Appendix 6 Recipes for TLC Stains.
Appendix 7 NMR Spectral Data of Common Contaminants of Organic and Organometallic Reaction Products.
Appendix 8 Acidities of Organic Functional Groups.
Appendix 9 Acidities of Organic Functional Groups in DMSO.
Appendix 10 Stuck Joints.
Index.

Handbook of Synthetic Organic Chemistry.css-1p8rvzy{position:absolute;padding-left:8px;}

Handbook of Synthetic Organic Chemistry